Comparison of Mass Spectrometry Sample Preparation Methods for Nylon 6,6 Analysis


BioChromato has published a technical note that compares using Evolved Gas Analysis (EGA) and Thermal Desorption (DART®) sample preparation methods for Mass Spectrometry analysis of Nylon 6,6.

 

Synthesized by polycondensation of hexamethylenediamine and adipic acid – Nylon 6,6 is a polyamide or nylon that is commonly used in the textile and plastic industries. Nylon 6,6 is a polymer of choice when high mechanical strength, rigidity, good stability under heat and/or chemical resistance are required. In this new technical note the authors compare ionRocket-DART®-MS to EGA-MS for analysis of Nylon 6,6 samples.

 

Evolved Gas Analysis has traditionally been used as a mass spectrometry sample preparation technique for polymers, plastics, and fibres. However, analysis by EGA-MS generates fragment ions and requires a database to confirm the identity of the mass fragments.

 

By comparison, the authors demonstrate how using ionRocket- DART®/MS you can observe the parent ion without fragment ions because DART® is a soft ionization technique. Consequently, ionRocket- DART®/MS can provide qualitative analysis even if customers cannot find an objective mass fragment within their EGA/MS database.

 

The ionRocket is a temperature-heating device for direct thermal desorption and pyrolysis of samples, prior to ionization and analysis by mass spectrometry. Using ionRocket a temperature gradient from ambient up to 600ºC can be achieved in just a few minutes. This enables polymers, plastics, and fibres to be pyrolyzed and then introduced into the DART®-MS gas stream.

 

This press release has been published in other Science Web sites as below;

Engineering Update, 9/2
Azom, 9/2
Automation Update, 9/2
Bio-Equip, 9/2
AzoSensors, 24/2
LabManager, 3/3
Labbulletin, 11/3
PresseBox, 24/2
Scientistlive NL, 9/3
NewsOnline24, 24/2
Scientistlive, 3/3
LabMate online, 1/3
Technology Networks, 1/3
Intl. LabMate, April, p.21
Chemistry World, April, p.67
Analytic Journal, 29/3
Analytic Journal (Ger), 29/3
Lab Asia, April, p.23

To download the press release in full in PDF format please click HERE.

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